Ethylmorpholine → HCID 58213447, compound

HRID 1897530Notes

Reaction equation

[CH2:1]([N:3]1[CH2:8][CH2:7][O:6][CH2:5][CH2:4]1)[CH3:2].[CH2:9]1[CH2:16][O:15][S:12](=[O:14])(=[O:13])[CH2:11][CH2:10]1>>[CH2:1]([N+:3]1([CH2:16][CH2:9][CH2:10][CH2:11][S:12]([O-:15])(=[O:14])=[O:13])[CH2:8][CH2:7][O:6][CH2:5][CH2:4]1)[CH3:2]

Participants

Reactant 2

HCID 7525Ethylmorpholine

HCID 154111,4-Butane sultone

Product 1

HCID 58213447HCID 58213447, compound

Procedure

1.15 grams of N-ethylmorpholine was alkylated with 1,4-butanesultone in similar fashion to the previous example to give 1.09 grams of a white solid. The structure was confirmed by positive mode electrospray mass spectroscopy (M+H)=252.6 and (M+Na) 274.2 m/z and 1H NMR.

Sources & evidence

ORD record: ord-7db2c68a7ba041eb9aa7f05ea17f6bbb
Source dataset: uspto-grants-2013_08
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US08519125B2

Reaction notes

Loading…