Benzoic Acid → HCID 12455494, compound

HRID 1899381Notes

Reaction equation

HRID 1899381 reaction equation
[CH:1]1[C:13]2[CH2:12][C:11]3[C:6](=[CH:7][CH:8]=[CH:9][CH:10]=3)[C:5]=2[CH:4]=[CH:3][CH:2]=1.[C:14]([OH:22])(=O)[C:15]1[CH:20]=[CH:19][CH:18]=[CH:17][CH:16]=1>>[C:14]([C:9]1[CH:8]=[CH:7][C:6]2[C:5]3[C:13](=[CH:1][C:2]([C:14](=[O:22])[C:15]4[CH:16]=[CH:17][CH:18]=[CH:19][CH:20]=4)=[CH:3][CH:4]=3)[CH2:12][C:11]=2[CH:10]=1)(=[O:22])[C:15]1[CH:20]=[CH:19][CH:18]=[CH:17][CH:16]=1

Participants

3

Reactant 2

HCID 243Benzoic AcidHCID 6853Fluorene2×

Product 1

HCID 12455494HCID 12455494, compound

Procedure

The compound 2,7-bis(dimethylphenylcarbyl) fluorene, which is believed to be a new compound, was prepared by reacting benzoic acid with fluorene in hot polyphosphoric acid at about 100° C. to yield 2,7-dibenzoylfluorene which is then reacted with trimethyl aluminum in boiling toluene.

Workup

  1. customwas prepared
  2. customat about 100° C.

Sources & evidence

ORD record
ord-bcaeeb4ef1d24b9983c9428d1e35163f
Source dataset
uspto-grants-1996_11
Patent number
US05571880

Reaction notes

Loading…