Hydrochloric Acid → HCID 178513444, compound

HRID 1902818Notes

Reaction equation

HRID 1902818 reaction equation
O.O.O.O.[Mn:5]([Cl:8])([Cl:7])=[O:6].[NH2:9][C:10]([NH2:12])=[O:11].O.Cl>>[OH2:6].[Mn:5]([Cl:8])([Cl:7])=[O:6].[NH2:9][C:10]([NH2:12])=[O:11]

Participants

5

Reactant 4

HCID 313Hydrochloric AcidHCID 962Water2×HCID 1176UreaHCID 178526979HCID 178526979, compound

Product 1

HCID 178513444HCID 178513444, compound

Procedure

In a 10 liter kettle is added 1005 g. (5.08 mole) manganous chloride tetrahydrate, 3600 g. (60.0 moles) urea, and 1800 g. (100 moles) water and warmed to 35° C. with stirring to dissolve to a clear pink solution of pH 7.3. To this is added 168 g. (1.68 mole) 36.5% hydrochloric acid and 233 g. (12.9 moles) water to yield 6806 g. of solution of pH 1.5.

Workup

  1. additionIn a 10 liter kettle is added 1005 g
  2. dissolutionto dissolve to a clear pink solution of pH 7.3
  3. additionTo this is added 168 g

Sources & evidence

ORD record
ord-b4feb89914e2496282edc1d72ea97ae8
Source dataset
uspto-grants-1982_12
Patent number
US04366096

Reaction notes

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