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HRID1903270

反应详情

EQUATION

反应方程式

HRID 1903270 的结构方程式

REACTANTS

反应物

2
结构：ICI
HCID6346

Methylene iodide

CH2I2

结构：Cc1ccc(C2=CCNC2)cc1
HCID3024855

未命名化合物

PRODUCTS

生成物

1
结构：Cc1ccc(C23CNCC2C3)cc1
HCID47953

1-(4-Methylphenyl)-3-azabicyclo[3.1.0]hexane

C12H15N

AUXILIARIES

试剂、催化剂与溶剂

2
结构：[Cu]
催化剂HCID23978

Copper

Cu

结构：c1ccccc1
溶剂HCID241

Benzene

C6H6

PROCEDURE

实验过程

A mixture of 3-(p-tolyl)-3-pyrroline, methylene iodide, and powdered copper in a molar ration of 1:2:4 is heated in benzene for about 50 hours. Filtration and evaporation of the solution gives 1-(p-tolyl)-3-azabicyclo[3.1.0]hexane.

WORKUP

后处理

  1. filtrationFiltration and evaporation of the solution