Triethylamine → HCID 14450290, compound

HRID 1904379Notes

Reaction equation

HRID 1904379 reaction equation
[NH2:1][C:2]1[C:7]([CH3:8])=[CH:6][C:5]([N:9]2[N:13]=[N:12][CH:11]=[N:10]2)=[CH:4][C:3]=1I.[C:15]([O-:19])(=[O:18])[CH:16]=[CH2:17].[CH2:20](N(CC)CC)[CH3:21]>C([O-])(=O)C.[Pd+2].C([O-])(=O)C>[NH2:1][C:2]1[C:7]([CH3:8])=[CH:6][C:5]([N:9]2[N:13]=[N:12][CH:11]=[N:10]2)=[CH:4][C:3]=1/[CH:17]=[CH:16]/[C:15]([O:19][CH2:20][CH3:21])=[O:18]

Participants

5

Reactant 3

HCID 8471TriethylamineHCID 25188AcrylateHCID 14450285HCID 14450285, compound

Product 1

HCID 14450290HCID 14450290, compound

Reagents, catalysts & solvents 1

HCID 167845palladium(II) acetateCatalyst

Procedure

The following compound, m.p. 162°-5°, was prepared similarly to the previous Preparation using 2-(4-amino-3-iodo-5-methylphenyl)tetrazole, ethyl, acrylate, palladium acetate and triethylamine as the starting materials: ##STR143##

Workup

  1. customThe following compound, m.p. 162°-5°, was prepared similarly to the previous Preparation

Sources & evidence

ORD record
ord-3f56b43516e941f69ef2effab10fbea2
Source dataset
uspto-grants-1989_06
Patent number
US04837334

Reaction notes

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