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HRID1907739

反应详情

EQUATION

反应方程式

HRID 1907739 的结构方程式

REACTANTS

反应物

3
结构：CC(=O)Oc1ccc(C(=O)O)cc1
HCID16865

4-Acetoxy benzoic acid

C9H8O4

结构：CN(C)[C@@H]1CCN(Cc2ccc(C(=O)O)cc2)C1
HCID59737509

未命名化合物

结构：CC(C)(C)OC(=O)Nc1ccc(C2=CC(=O)CC2)cc1N
HCID59737590

未命名化合物

PRODUCTS

生成物

1
结构：CC(=O)Oc1ccc(C(=O)Nc2cc(C3=CC(=O)CC3)ccc2NC(=O)OC(C)(C)C)cc1
HCID59737207

未命名化合物

收率 30%

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CCOC(C)=O
溶剂HCID8857

Ethyl acetate

C4H8O2

PROCEDURE

实验过程

Following the same procedure as described in Example 1, step 6 (scheme 1), but substituting compound 4 for compound 258 and compound 7 for 4-acetoxybenzoic acid, title compound 259 was obtained as a yellow oil in 30% yield [after flash chromatography (eluent: 30% AcOEt in hexanes)].