HRID1910680
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
AUXILIARIES
试剂、催化剂与溶剂
PROCEDURE
实验过程
2-(tert-Butoxycarbonylamino)-4-(2-chlorophenyl)butanoic acid (2.25 g) was dissolved in 4 N HCl in dioxane (20 mL, 11 eq) and stirred at room temperature for 1 h. The solution was then concentrated delivering product as a yellow solid (1.49 g, 83% yield).
WORKUP
后处理
- concentrationThe solution was then concentrated