Hydroxylamine → 3-Pyridine aldoxime

HRID 1913354Notes

Reaction equation

HRID 1913354 reaction equation
[CH:1](=O)[C:2]1[CH:7]=[CH:6][CH:5]=[N:4][CH:3]=1.[NH2:9][OH:10].C([O-])(=O)C.[Na+]>C(O)C>[CH:1](=[N:9][OH:10])[C:2]1[CH:7]=[CH:6][CH:5]=[N:4][CH:3]=1

Participants

5

Reactant 3

HCID 787HydroxylamineHCID 103713-PyridinecarboxaldehydeHCID 517045Sodium Acetate

Product 1

HCID 6943-Pyridine aldoxime

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

Nicotinaldehyde oxime was prepared in quantitative yield by the reaction of nicotinaldehyde with hydroxylamine and sodium acetate in ethanol as for 20.

Sources & evidence

ORD record
ord-3ac64effe1654cf0a711538f66f00e62
Source dataset
uspto-grants-2013_12
Patent number
US08609708B2

Reaction notes

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