HRID1914512
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
AUXILIARIES
试剂、催化剂与溶剂
PROCEDURE
实验过程
[2-benzylsulfanyl-6-(4-trifluoromethyl-phenyl)-pyrimidin-4-ylmethyl]-carbamic acid tert-butyl ester was diluted with 4N HCl in dioxane (20 mL) at rt. After 30 min. the mixture was concentrated and the resulting solid was used without further purification. MS (ESI): mass calcd. for C19H16F3N3S, 373.2; m/z found, 374.2 [M+H]+.
WORKUP
后处理
- concentrationAfter 30 min. the mixture was concentrated
- customthe resulting solid was used without further purification