HRID1914512

反应详情

EQUATION

反应方程式

HRID 1914512 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

[2-benzylsulfanyl-6-(4-trifluoromethyl-phenyl)-pyrimidin-4-ylmethyl]-carbamic acid tert-butyl ester was diluted with 4N HCl in dioxane (20 mL) at rt. After 30 min. the mixture was concentrated and the resulting solid was used without further purification. MS (ESI): mass calcd. for C19H16F3N3S, 373.2; m/z found, 374.2 [M+H]+.

WORKUP

后处理

  1. concentrationAfter 30 min. the mixture was concentrated
  2. customthe resulting solid was used without further purification