Dimethylformamide dimethyl acetal → HCID 68462393, compound

HRID 1915543Notes

Reaction equation

HRID 1915543 reaction equation
[CH3:1][O:2][CH:3]([O:19][CH3:20])[C:4]1[CH:9]=[CH:8][C:7]([C:10](=[O:18])[CH2:11][C:12]2[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=2)=[CH:6][CH:5]=1.CO[CH:23](OC)[N:24]([CH3:26])[CH3:25]>CN(C=O)C>[CH3:20][O:19][CH:3]([O:2][CH3:1])[C:4]1[CH:5]=[CH:6][C:7]([C:10](=[O:18])[C:11]([C:12]2[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=2)=[CH:23][N:24]([CH3:26])[CH3:25])=[CH:8][CH:9]=1

Participants

4

Reactant 2

HCID 78373Dimethylformamide dimethyl acetalHCID 53434070HCID 53434070, compound

Product 1

HCID 68462393HCID 68462393, compound

Reagents, catalysts & solvents 1

HCID 6228DimethylformamideSolvent

Procedure

5 g 1-[4-(dimethoxymethyl)phenyl]-2-phenylethanone and 4.43 g N,N-dimethylformamid dimethylacetal are stirred for 18 h at 100° C. in DMF. The solvent is removed and the crude product used without further purification.

Workup

  1. customThe solvent is removed
  2. customthe crude product used without further purification

Sources & evidence

ORD record
ord-3d66a0fdddd44b1683d33be754876c91
Source dataset
uspto-grants-2013_12
Patent number
US08614218B2

Reaction notes

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