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HRID1929844

反应详情

EQUATION

反应方程式

HRID 1929844 的结构方程式

REACTANTS

反应物

2
结构：Oc1ccccc1Cl
HCID7245

2-Chlorophenol

C6H5ClO

结构：O=C(N[C@@H]1CCCC[C@H]1O)c1cnc(Br)c(-c2ccc(Cl)cc2)n1
HCID86616972

未命名化合物

PRODUCTS

生成物

1
结构：O=C(N[C@@H]1CCCC[C@H]1O)c1cnc(Oc2ccccc2Cl)c(-c2ccc(Cl)cc2)n1
HCID24857248

未命名化合物

PROCEDURE

实验过程

The title compound was synthesized in analogy to the procedure described for the preparation of Example 36 c, using 5-bromo-6-(4-chloro-phenyl)-pyrazine-2-carboxylic acid ((1R,2R)-2-hydroxy-cyclohexyl)-amide, and chlorophenol (commercially available) as starting materials to give the title compound as a white solid. mp.: 154-155° C., MS (ISP): 458.3, 460.3 (M+H)+.

WORKUP

后处理

  1. customThe title compound was synthesized in analogy to the procedure
  2. customdescribed for the preparation of Example 36 c