Hydrochloric Acid → HCID 86615259, compound

HRID 1932376Notes

Reaction equation

HRID 1932376 reaction equation
[F:1][C:2]1[CH:7]=[N:6][C:5]([NH:8][CH2:9][CH2:10][C:11]2[CH:18]=[CH:17][CH:16]=[CH:15][C:12]=2[CH:13]=[O:14])=[C:4]2[NH:19][C:20]([CH3:23])=[C:21]([CH3:22])[C:3]=12.[ClH:24]>C(OCC)(=O)C>[ClH:24].[F:1][C:2]1[CH:7]=[N:6][C:5]([NH:8][CH2:9][CH2:10][C:11]2[CH:18]=[CH:17][CH:16]=[CH:15][C:12]=2[CH:13]=[O:14])=[C:4]2[NH:19][C:20]([CH3:23])=[C:21]([CH3:22])[C:3]=12

Participants

4

Reactant 2

HCID 313Hydrochloric AcidHCID 86615260HCID 86615260, compound

Product 1

HCID 86615259HCID 86615259, compound

Reagents, catalysts & solvents 1

HCID 8857Ethyl AcetateSolvent

Procedure

A solution of the compound (5 mg) prepared in Step 1 in ethyl acetate was saturated with hydrochloric acid gas and then filtered to give 2.3 mg of the titled compound as a pale yellow solid.

Workup

  1. filtrationfiltered

Sources & evidence

ORD record
ord-1169403e37a04242aba501eda4f6f129
Source dataset
uspto-grants-2012_05
Patent number
US08188114B2

Reaction notes

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