Potassium Carbonate → HCID 15549922, compound

HRID 1935561Notes

Reaction equation

HRID 1935561 reaction equation
[CH:1]1([NH:4][CH:5]=[C:6]([C:12](=[O:25])[C:13]2[CH:18]=[C:17]([N+:19]([O-:21])=[O:20])[C:16]([F:22])=[C:15]([Cl:23])[C:14]=2F)[C:7]([O:9][CH2:10][CH3:11])=[O:8])[CH2:3][CH2:2]1.C(=O)([O-])[O-].[K+].[K+]>C(OCC)(=O)C>[CH:1]1([N:4]2[C:14]3[C:13](=[CH:18][C:17]([N+:19]([O-:21])=[O:20])=[C:16]([F:22])[C:15]=3[Cl:23])[C:12](=[O:25])[C:6]([C:7]([O:9][CH2:10][CH3:11])=[O:8])=[CH:5]2)[CH2:3][CH2:2]1

Participants

4

Reactant 2

HCID 11430Potassium CarbonateHCID 178471885HCID 178471885, compound

Product 1

HCID 15549922HCID 15549922, compound

Reagents, catalysts & solvents 1

HCID 8857Ethyl AcetateSolvent

Procedure

An amount of 0.088 g of ethyl 3-cyclopropylamino-2-(2,4-difluoro-3-chloro-5-nitro-benzoyl)acrylate is dissolved in 1 ml of ethyl acetate at 0° C . A quantity of 0.1 g of potassium carbonate is added. The desired product precipitates and is isolated by filtration.

Workup

  1. customThe desired product precipitates
  2. customis isolated by filtration

Sources & evidence

ORD record
ord-27b72b7987a24a2eb7eabfb333a14998
Source dataset
uspto-grants-2002_05
Patent number
US06387928B1

Reaction notes

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