Piperidine → HCID 178439936, compound

HRID 1937897Notes

Reaction equation

HRID 1937897 reaction equation
C1CCNCC1.CCCc1nc2ccc(I)cc2c(=O)n1Cc1ccc(-c2ccccc2S(=O)(=O)NC(C)(C)C)cc1>C1COCCO1.CC(C)Oc1cccc(OC(C)C)c1-c1ccccc1P(C1CCCCC1)C1CCCCC1.C[Si](C)(C)[N-][Si](C)(C)C.Nc1ccccc1-c1[c-]cccc1.[Cl][Pd+].[Li+]>CCCc1nc2ccc(N3CCCCC3)cc2c(=O)n1Cc1ccc(-c2ccccc2S(=O)(=O)NC(C)(C)C)cc1

Participants

6

Reactant 2

HCID 8082PiperidineHCID 132556033HCID 132556033, compound

Product 1

HCID 178439936HCID 178439936, compoundYield 39%

Reagents, catalysts & solvents 3

HCID 2733832Lithium HexamethyldisilazideReagentHCID 771465301375325-68-0CatalystHCID 312751,4-DioxaneSolvent2×

Conditions

Temperature
80 °C

Workup

  1. additionNo procedure recorded

Sources & evidence

ORD record
ord-d2ac0353a3a54805a2040995757d1d3d
Source dataset
Pd_CN_Coupling_Informer_Library
Original link
View source

Reaction notes

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