Piperidine → HCID 178473333, compound

HRID 1937906Notes

Reaction equation

HRID 1937906 reaction equation
C1CCNCC1.CCOC(=O)N1CCC(=C2c3ccc(Cl)cc3CCc3cc(Br)cnc32)CC1>CC(C)(C)O.CC(C)Oc1cccc(OC(C)C)c1-c1ccccc1P(C1CCCCC1)C1CCCCC1.Nc1ccccc1-c1[c-]cccc1.O=C([O-])[O-].[Cl][Pd+].[K+].[K+]>CCOC(=O)N1CCC(=C2c3ccc(Cl)cc3CCc3cc(N4CCCCC4)cnc32)CC1

Participants

6

Reactant 2

HCID 8082PiperidineHCID 10742688Ethyl 4-(3-bromo-8-chloro-5,6-dihydro-11H-benzo[5,6]cyclohepta[1,2-b]pyridin-11-ylidene)piperidine-1-carboxylate

Product 1

HCID 178473333HCID 178473333, compoundYield 63%

Reagents, catalysts & solvents 3

HCID 11430Potassium CarbonateReagentHCID 771465301375325-68-0CatalystHCID 6386tert-ButanolSolvent2×

Conditions

Temperature
80 °C

Workup

  1. additionNo procedure recorded

Sources & evidence

ORD record
ord-30d1c9a1f152483596b1701e230ece29
Source dataset
Pd_CN_Coupling_Informer_Library
Original link
View source

Reaction notes

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