Diethylamine → HCID 11858098, compound

HRID 1939959Notes

Reaction equation

[C:1]([C:3]1[CH:8]=[CH:7][C:6]([OH:9])=[CH:5][CH:4]=1)#[N:2].Br[CH2:11][CH2:12][CH2:13][CH2:14]Cl.[CH2:16]([NH:18][CH2:19][CH3:20])[CH3:17]>>[CH2:16]([N:18]([CH2:19][CH3:20])[CH2:11][CH2:12][CH2:13][CH2:14][O:9][C:6]1[CH:7]=[CH:8][C:3]([C:1]#[N:2])=[CH:4][CH:5]=1)[CH3:17]

Participants

Reactant 3

HCID 8021Diethylamine

HCID 130194-Cyanophenol

HCID 813641-Bromo-4-chlorobutane

Product 1

HCID 11858098HCID 11858098, compound

Procedure

According to a similar manner as that in Reference Example 78 except that 4-cyanophenol, 1-bromo-4-chlorobutane, and diethylamine were used, 4-[4-(diethylamino)butoxy]benzonitrile (quantitative) was obtained as a crude product.

Sources & evidence

ORD record: ord-529b826be83247668d53756f7b0b5464
Source dataset: uspto-grants-1997_12
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US05698560

Reaction notes

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