Chloroacetonitrile → HCID 21460388, compound

HRID 1941210Notes

Reaction equation

HRID 1941210 reaction equation
[CH2:1]([O:8][CH2:9][CH2:10][NH2:11])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[CH2:12]([N:14](CC)CC)[CH3:13].ClCC#N>O1CCCC1>[CH2:1]([O:8][CH2:9][CH2:10][NH:11][CH2:13][C:12]#[N:14])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1

Participants

5

Reactant 3

HCID 7856ChloroacetonitrileHCID 8471TriethylamineHCID 5338682-(Benzyloxy)ethanamine

Product 1

HCID 21460388HCID 21460388, compound

Reagents, catalysts & solvents 1

HCID 8028TetrahydrofuranSolvent

Procedure

A mixture of 2-benzyloxyethylamine (40 g) and triethylamine (50 ml) in tetrahydrofuran (500 ml) was treated dropwise with chloroacetonitrile (23 g) at room temperature.

Sources & evidence

ORD record
ord-618f8ffd230144aaa845bb6b269066be
Source dataset
uspto-grants-1997_12
Patent number
US05703087

Reaction notes

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