HRID1942365

反应详情

EQUATION

反应方程式

HRID 1942365 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

To a mixture of 3.15 g (30 mmol) 2,2-dimethoxy-ethylamine and 40 mL dioxane is added 1.91 g (10 mmol) naphthalene-2-carbonyl chloride. After stirring overnight the solution is pored into 200 mL of ice water. Filtration yields the product in almost quantitative yield as a white solid.

WORKUP

后处理

  1. filtrationFiltration
  2. customyields the product in almost quantitative yield as a white solid