Triethylamine → HCID 178484863, compound

HRID 1946940Notes

Reaction equation

HRID 1946940 reaction equation
[OH:1][C@H:2]1[CH2:7][CH2:6][C@@H:5]([NH:8][CH3:9])[CH2:4][CH2:3]1.[CH3:10][S:11](Cl)(=[O:13])=[O:12].C(N(CC)CC)C>O1CCCC1>[CH3:10][S:11]([O:1][C@H:2]1[CH2:7][CH2:6][C@@H:5]([N:8]([S:11]([CH3:10])(=[O:13])=[O:12])[CH3:9])[CH2:4][CH2:3]1)(=[O:13])=[O:12]

Participants

5

Reactant 3

HCID 8471TriethylamineHCID 31297Methanesulfonyl chlorideHCID 178484842HCID 178484842, compound

Product 1

HCID 178484863HCID 178484863, compound

Reagents, catalysts & solvents 1

HCID 8028TetrahydrofuranSolvent

Procedure

Prepared by reacting cis-1-hydroxy-4-methylamino-cyclohexane with methanesulphonic acid chloride in tetrahydrofuran in the presence of triethylamine.

Workup

  1. customPrepared

Sources & evidence

ORD record
ord-3e2323f0f4064c4fbba314287e072807
Source dataset
uspto-grants-2013_03
Patent number
US08399461B2

Reaction notes

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