HRID1950749

反应详情

EQUATION

反应方程式

HRID 1950749 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

0.57 g 1-cyclopropyl-4-(4-nitro-phenyl)-piperidine are dissolved in 30 mL tetrahydrofuran and combined with Pd/C. The mixture is hydrogenated for 72 h at 7 bar hydrogen pressure. Then the catalyst is filtered off and the solvent is eliminated in vacuo. The residue is used in the next stage of the synthesis without any further purification.

WORKUP

后处理

  1. filtrationThen the catalyst is filtered off
  2. customThe residue is used in the next stage of the synthesis without any further purification