Hydrochloric Acid → HCID 88177698, compound

HRID 1952797Notes

Reaction equation

HRID 1952797 reaction equation
[ClH:1].[CH3:2][N:3]([CH3:33])[CH2:4][CH2:5][CH2:6][NH:7][C:8]([O:10][CH2:11][C:12]1[CH:17]=[CH:16][CH:15]=[CH:14][C:13]=1[N:18]([CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][CH2:26][CH2:27][CH2:28][CH2:29][CH2:30][CH2:31][CH3:32])[CH:19]=[O:20])=[O:9]>C(OCC)(=O)C>[ClH:1].[CH3:33][N:3]([CH3:2])[CH2:4][CH2:5][CH2:6][NH:7][C:8]([O:10][CH2:11][C:12]1[CH:17]=[CH:16][CH:15]=[CH:14][C:13]=1[N:18]([CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][CH2:26][CH2:27][CH2:28][CH2:29][CH2:30][CH2:31][CH3:32])[CH:19]=[O:20])=[O:9]

Participants

4

Reactant 2

HCID 313Hydrochloric AcidHCID 54415483HCID 54415483, compound

Product 1

HCID 88177698HCID 88177698, compound

Reagents, catalysts & solvents 1

HCID 8857Ethyl AcetateSolvent2×

Procedure

4N Hydrochloric acid--ethyl acetate solution (0.13 ml) was added to a solution of [2-[[N-[3-(dimethylamino)propyl]carbamoyloxy]methyl]phenyl]-N-dodecylformamide (0.200 g) in ethyl acetate (2 ml) at room temperature. After being stirred for 15 minutes, the reaction mixture was concentrated, thereby yielding 0.217 g of the aimed compound as white solid.

Workup

  1. concentrationthe reaction mixture was concentrated

Sources & evidence

ORD record
ord-af4efa3d179b4c3f800f6a6e5e1ed9f4
Source dataset
uspto-grants-2000_09
Patent number
US06114325

Reaction notes

Loading…