Hydrochloric Acid → HCID 88176300, compound

HRID 1952798Notes

Reaction equation

HRID 1952798 reaction equation
[ClH:1].[CH2:2]([N:12]([C:15]1[CH:20]=[CH:19][CH:18]=[CH:17][C:16]=1[CH2:21][O:22][C:23](=[O:31])[NH:24][CH2:25][CH2:26][CH2:27][N:28]([CH3:30])[CH3:29])[CH:13]=[O:14])[CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH3:11]>C(OCC)(=O)C>[ClH:1].[CH2:2]([N:12]([C:15]1[CH:20]=[CH:19][CH:18]=[CH:17][C:16]=1[CH2:21][O:22][C:23](=[O:31])[NH:24][CH2:25][CH2:26][CH2:27][N:28]([CH3:30])[CH3:29])[CH:13]=[O:14])[CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH3:11]

Participants

4

Reactant 2

HCID 313Hydrochloric AcidHCID 57304311HCID 57304311, compound

Product 1

HCID 88176300HCID 88176300, compound

Reagents, catalysts & solvents 1

HCID 8857Ethyl AcetateSolvent2×

Procedure

4N Hydrochloric acid--ethyl acetate solution (0.14 ml) was added to a solution of N-decyl-[2-[[N-[3-(dimethylamino)propyl]carbamoyloxy]methyl]phenyl]formamide (0.200 g) in ethyl acetate (2 ml) at room temperature. After being stirred for 10 minutes, the reaction mixture was concentrated, thereby yielding 0.209 g of the aimed compound as white syrup.

Workup

  1. concentrationthe reaction mixture was concentrated

Sources & evidence

ORD record
ord-7b324c9ed78d45fcb253c8dfd9eb5a22
Source dataset
uspto-grants-2000_09
Patent number
US06114325

Reaction notes

Loading…