Potassium Carbonate → HCID 23296619, compound

HRID 1954377Notes

Reaction equation

HRID 1954377 reaction equation
[C:1]([C:3]1[CH:8]=[CH:7][C:6]([CH2:9][CH2:10][C:11]2[O:12][C:13]3[CH:19]=[C:18]([NH:20][S:21]([C:24]4[CH:25]=[CH:26][CH:27]=[C:28]5[C:33]=4[N:32]=[CH:31][CH:30]=[CH:29]5)(=[O:23])=[O:22])[CH:17]=[CH:16][C:14]=3[N:15]=2)=[CH:5][CH:4]=1)#[N:2].Br[CH2:35][C:36]([O:38][CH3:39])=[O:37].C(=O)([O-])[O-].[K+].[K+]>CC(C)=O>[C:1]([C:3]1[CH:8]=[CH:7][C:6]([CH2:9][CH2:10][C:11]2[O:12][C:13]3[CH:19]=[C:18]([N:20]([S:21]([C:24]4[CH:25]=[CH:26][CH:27]=[C:28]5[C:33]=4[N:32]=[CH:31][CH:30]=[CH:29]5)(=[O:23])=[O:22])[CH2:35][C:36]([O:38][CH3:39])=[O:37])[CH:17]=[CH:16][C:14]=3[N:15]=2)=[CH:5][CH:4]=1)#[N:2]

Participants

5

Reactant 3

HCID 11430Potassium CarbonateHCID 60984Methyl bromoacetateHCID 23296426HCID 23296426, compound

Product 1

HCID 23296619HCID 23296619, compound

Reagents, catalysts & solvents 1

HCID 180AcetoneSolvent

Procedure

Prepared analogously to Example 1d from 2-[2-(4-cyanophenyl)-ethyl]-6-[N-quinoline-8-sulphonylamino]-benzoxazole, methyl bromoacetate and potassium carbonate in acetone.

Sources & evidence

ORD record
ord-340b5e42e5b2446eac7a41b92c6afa39
Source dataset
uspto-grants-2000_09
Patent number
US06121308

Reaction notes

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