Cyanuric chloride → HCID 19069531, compound

HRID 1957292Notes

Reaction equation

HRID 1957292 reaction equation
[CH3:1][O:2][CH:3]([O:6][CH3:7])[CH2:4][NH2:5].[N:8]1[C:15](Cl)=[N:14][C:12](Cl)=[N:11][C:9]=1Cl>>[CH3:1][O:2][CH:3]([O:6][CH3:7])[CH2:4][NH:5][C:9]1[N:11]=[C:12]([NH:5][CH2:4][CH:3]([O:6][CH3:7])[O:2][CH3:1])[N:14]=[C:15]([NH:5][CH2:4][CH:3]([O:6][CH3:7])[O:2][CH3:1])[N:8]=1

Participants

3

Reactant 2

HCID 7954Cyanuric chlorideHCID 89728Aminoacetaldehyde dimethyl acetal

Product 1

HCID 19069531HCID 19069531, compound

Procedure

The procedure of Example 1 was repeated with the exception that aminoacetaldehyde dimethyl acetal (6.3 g, 0.060 mole) and cyanuric chloride (3.68 g, 0.02 mole) were used to give 2,4,6-tris-(2,2-dimethoxyethylamino)-1,3,5-triazine as an oily product in 80.8% isolated yield (6.3g). The structure was analyzed by infrared (IR) spectroscopy, and confirmed by NMR spectroscopy 1H NMR (δ): 4.2 (t, 1H), 3.6-3.2 (m, 2H), 3.4 (s, 6H).

Sources & evidence

ORD record
ord-5b72c5986a614d2fbf0f872af4f51c27
Source dataset
uspto-grants-1998_07
Patent number
US05783642

Reaction notes

Loading…