Methane → HCID 58288501, compound

HRID 1969097Notes

Reaction equation

HRID 1969097 reaction equation
[CH2:1]([O:3][C:4](=[O:33])[CH2:5][C:6]1[CH:11]=[CH:10][C:9]([O:12][CH3:13])=[C:8]([O:14][C:15]2[CH:20]=[CH:19][C:18]([N+:21]([O-])=O)=[CH:17][C:16]=2[CH2:24][N:25]([C:28]([CH:30]2[CH2:32][CH2:31]2)=[O:29])[CH2:26][CH3:27])[CH:7]=1)[CH3:2].CN(C)N.C>>[CH2:1]([O:3][C:4](=[O:33])[CH2:5][C:6]1[CH:11]=[CH:10][C:9]([O:12][CH3:13])=[C:8]([O:14][C:15]2[CH:20]=[CH:19][C:18]([NH2:21])=[CH:17][C:16]=2[CH2:24][N:25]([C:28]([CH:30]2[CH2:31][CH2:32]2)=[O:29])[CH2:26][CH3:27])[CH:7]=1)[CH3:2]

Participants

4

Reactant 3

HCID 297MethaneHCID 59761,1-DimethylhydrazineHCID 58288502HCID 58288502, compound

Product 1

HCID 58288501HCID 58288501, compound

Procedure

Prepared according to the procedure described in Example 42, Step 4, using the following starting materials: (3-{2-[(cyclopropanecarbonyl-ethyl-amino)-methyl]-4-nitro-phenoxy}-4-methoxy-phenyl)-acetic acid ethyl ester, 1,1-dimethylhydrazine, ferric chloride, and DARCO.

Workup

  1. customPrepared

Sources & evidence

ORD record
ord-8c502317cd634a5c98de002d5156516b
Source dataset
uspto-grants-2013_04
Patent number
US08426449B2

Reaction notes

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