Hydrochloric Acid → HCID 130172856, compound

HRID 1969147Notes

Reaction equation

HRID 1969147 reaction equation
[OH:1][N:2]=[CH:3][C:4]1[CH:5]=[CH:6][C:7]([O:12][CH3:13])=[C:8]([CH:11]=1)[C:9]#[N:10].[ClH:14]>CN(C=O)C>[C:9]([C:8]1[CH:11]=[C:4]([C:3]([Cl:14])=[N:2][OH:1])[CH:5]=[CH:6][C:7]=1[O:12][CH3:13])#[N:10]

Participants

4

Reactant 2

HCID 313Hydrochloric AcidHCID 77066184HCID 77066184, compound

Product 1

HCID 130172856HCID 130172856, compound

Reagents, catalysts & solvents 1

HCID 6228DimethylformamideSolvent

Procedure

5-[(Hydroxyimino)methyl]-2-methoxybenzonitrile, 4 M hydrochloric acid and Oxon (registered trade name) were dissolved in a DMF solution, followed by stirring at room temperature for 12 hours to obtain 3-cyano-N-hydroxy-4-methoxybenzenecaboximidoyl chloride. NMRC: 7.01 (1H, d), 8.03 (1H, dd), 8.07 (1H, d).

Sources & evidence

ORD record
ord-39e16798523641659f534d3361baa19a
Source dataset
uspto-grants-2013_04
Patent number
US08426453B2

Reaction notes

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