Hydrochloric Acid → HCID 131730528, compound

HRID 1970085Notes

Reaction equation

[CH2:1]([NH2:5])[CH2:2][CH2:3][CH3:4].CO[Si:8](OC)(OC)[CH2:9][CH2:10][CH2:11][Cl:12].Cl>>[ClH:12].[CH2:1]([NH:5][CH2:11][CH2:10][CH2:9][SiH3:8])[CH2:2][CH2:3][CH3:4]

Participants

Reactant 3

HCID 313Hydrochloric Acid

HCID 8007Butylamine3×

HCID 624493-(Trimethoxysilyl)propyl chloride

Product 1

HCID 131730528HCID 131730528, compound

Procedure

A reaction of n-butylamine with CPTMO with a ratio of 3:1 consumes 1 mol of n-butylamine. 2 moles of n-butylamine can be removed again by distillation without any addition. This is because the reaction forms 1 mol of HCl, and, as a result of the distillation, 1 mol of n-butylaminopropylsilane hydrochloride is present at the end of the reaction.

Sources & evidence

ORD record: ord-e78391a238354302a14679684597bfd8
Source dataset: uspto-grants-2013_04
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US08426628B2

Reaction notes

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