HRID1970510

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID7504

Benzylamine

C7H9N

HCID81531

Diisopropylethylamine

C8H19N

结构：CC(C)(C)OC(=O)N[C@@H](CCC(=O)O)C(=O)OCc1ccccc1

HCID153708

tert-Butyloxycarbonyl-glutamic acid 1-benzyl ester

C17H23NO6

结构：CN(C)C(On1nnc2cccnc21)=[N+](C)C.F[P-](F)(F)(F)(F)F

HCID9886157

Methanaminium, N-((dimethylamino)(3H-1,2,3-triazolo(4,5-b)pyridin-3-yloxy)methylene)-N-methyl-, hexafluorophosphate(1-) (1:1)

C10H15F6N6OP

PRODUCTS

生成物

结构：CC(C)(C)OC(=O)N[C@@H](CCC(=O)NCc1ccccc1)C(=O)OCc1ccccc1

HCID15674275

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

溶剂HCID6228

N,N-Dimethylformamide

C3H7NO

PROCEDURE

实验过程

To a solution of 1.00 g (S)-2-tert-butoxycarbonylamino-pentanedioic acid 1-benzyl ester in 15 ml DMF were added 1.24 g HATU, 1.1 ml DIPEA and 0.32 ml benzylamine at 0° C.