HRID1974226

反应详情

EQUATION

反应方程式

HRID 1974226 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

3

PROCEDURE

实验过程

By a procedure similar to that of Example I, the above compound (3.9 g., m.p. 170°-173° C.) was prepared from 3.8 g. (0.025 m.) of p-hydroxyphenylisothiocyanate and 3.2 g. (0.025 m.) of cyclohexylisocyanate, using 50 mls. of benzene as a solvent and 3 drops each of triethylamine and dibutyltin dilaurate as catalysts.

WORKUP

后处理

  1. customBy a procedure similar to that of Example I, the above compound (3.9 g., m.p. 170°-173° C.) was prepared from 3.8 g