Hexachloroethane → HCID 14949193, compound

HRID 1975846Notes

Reaction equation

HRID 1975846 reaction equation
[Cl:1]C(Cl)(Cl)C(Cl)(Cl)Cl.C1(P(C2C=CC=CC=2)C2C=CC=CC=2)C=CC=CC=1.C(N(CC)CC)C.[CH3:35][Si:36]([CH3:48])([CH3:47])[NH:37][S:38]([C:41]1[CH:46]=[CH:45][CH:44]=[CH:43][CH:42]=1)(=O)=[O:39]>>[CH3:35][Si:36]([CH3:48])([CH3:47])[N:37]=[S:38]([Cl:1])([C:41]1[CH:46]=[CH:45][CH:44]=[CH:43][CH:42]=1)=[O:39]

Participants

5

Reactant 4

HCID 6214HexachloroethaneHCID 8471TriethylamineHCID 11776TriphenylphosphineHCID 12271451N-(Trimethylsilyl)benzenesulfonamide

Product 1

HCID 14949193HCID 14949193, compound

Procedure

The reactants used in the general procedure were hexachloroethane (0.1353 mol, 32.68 g), triphenylphosphine (0.1367 mol, 36.22 g), triethylamine (0.1353 mol, 19.2 ml), and N-trimethylsilyl-sulfonamide (3b) (0.1353 mol, 31.0 g).

Sources & evidence

ORD record
ord-75622fd6ff1a4980a05dc4baccb973cb
Source dataset
uspto-grants-1994_02
Patent number
US05288893

Reaction notes

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