Toluene → HCID 131722564, compound

HRID 1977452Notes

Reaction equation

HRID 1977452 reaction equation
[CH3:1][C:2]1[CH:8]=[C:7]([C:9]([C:12]2[CH:17]=[CH:16][C:15]([OH:18])=[CH:14][CH:13]=2)([CH3:11])[CH3:10])[CH:6]=[CH:5][C:3]=1[OH:4].C(=O)([O-])[O-].[K+].[K+].F[C:26]1[CH:40]=[CH:39][C:29]([C:30]([C:32]2[CH:37]=[CH:36][C:35](F)=[CH:34][CH:33]=2)=[O:31])=[CH:28][CH:27]=1.C1(C)C=CC=CC=1>CN(C)C(=O)C>[CH3:1][C:2]1[CH:8]=[C:7]([C:9]([C:12]2[CH:13]=[CH:14][C:15]([OH:18])=[CH:16][CH:17]=2)([CH3:11])[CH3:10])[CH:6]=[CH:5][C:3]=1[OH:4].[C:30]([C:32]1[CH:37]=[CH:36][CH:35]=[CH:34][CH:33]=1)(=[O:31])[C:29]1[CH:39]=[CH:40][CH:26]=[CH:27][CH:28]=1

Participants

6

Reactant 4

HCID 1140TolueneHCID 95824,4'-DifluorobenzophenoneHCID 11430Potassium CarbonateHCID 143890094-[2-(4-Hydroxyphenyl)propan-2-yl]-2-methylphenol

Product 1

HCID 131722564HCID 131722564, compound

Reagents, catalysts & solvents 1

HCID 31374DimethylacetamideSolvent

Procedure

Polymerization was carried out similar to the P(BPZ-BNZPH) polymerization, except methylbisphenol-A (10.0000 g, 39.00 mmol), potassium carbonate (10.782 g, 78.00 mmol), 4,4′-difluorobenzophenone (8.5102 g, 39.00 mmol), toluene (50 g) and N,N-dimethylacetamide (85 g) were used. The yield was about 15.34 g. The number average molecular weight of the polymer was about 8.2 K.

Workup

  1. customPolymerization
  2. customwas about 8.2 K

Sources & evidence

ORD record
ord-9d859885dea54ff7a7f6917f5b86f3ba
Source dataset
uspto-grants-2001_05
Patent number
US06232025B1

Reaction notes

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