HRID1978409
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
AUXILIARIES
试剂、催化剂与溶剂
PROCEDURE
实验过程
In 1 ml of methanol was dissolved 0.452 g of (R)-N-[1-(1,4-benzodioxan-2-ylmethyl)piperidin-4-ylmethyl]-5-thia-1,8b-diazaacenaphthylene-4-carboxamide, followed by addition of an excess of methanolic HCl. The mixture was stirred and concentrated to provide the title compound.
WORKUP
后处理
- concentrationconcentrated