HRID1986538

反应详情

EQUATION

反应方程式

HRID 1986538 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

460 mg of 30 (1.235 mmol) are taken up in a 25 ml round-bottomed flask and 9.3 ml of a solution of hydrogen chloride in dioxane (4M) are added. The medium is stirred for 4 hours at room temperature under argon. After evaporating off the solvent, 460 mg of amine 31 are obtained in hydrochloride form, which product is used directly in the following step.

WORKUP

后处理

  1. customAfter evaporating off the solvent, 460 mg of amine 31
  2. customare obtained in hydrochloride form, which product