HRID1986542
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
AUXILIARIES
试剂、催化剂与溶剂
PROCEDURE
实验过程
230 mg of 36 (0.57 mmol) are taken up in a 25 ml round-bottomed flask and 3 ml of a solution of hydrogen chloride in dioxane (4M) are added. The mixture is stirred for 2 hours at room temperature under argon. After evaporating off the solvent, 290 mg of amine 37 are obtained in hydrochloride form, which product is used directly in the following step.
WORKUP
后处理
- customAfter evaporating off the solvent, 290 mg of amine 37
- customare obtained in hydrochloride form, which product