HRID1986546

反应详情

EQUATION

反应方程式

HRID 1986546 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

510 mg of 42 (1.32 mmol) are taken up in a 25 ml round-bottomed flask and 10 ml of a solution of hydrogen chloride in dioxane (4M) are added. The mixture is stirred for 3 hours at room temperature under argon. After evaporating off the solvent, 510 mg of amine 43 are obtained in hydrochloride form, which product is used directly in the following step.

WORKUP

后处理

  1. customAfter evaporating off the solvent, 510 mg of amine 43
  2. customare obtained in hydrochloride form, which product