反应详情

A mixture of Z-N-Me-Val-N-Me-Tyr(3-t-Bu)-NHSO2Me (0.65 g, 1.13 mmol) and 20% palladium hydroxide/carbon (0.09 g) in methanol (10 ml) was stirred at room temperature for 2.5 hours in a hydrogen atmosphere. The reaction mixture was filtered and the filtrate was evaporated to remove the solvent under reduced pressure, giving crude N-Me-Val-N-Me-Tyr(3-t-Bu)-NHSO2Me (0.50 g).

1. filtrationThe reaction mixture was filtered
2. customthe filtrate was evaporated
3. customto remove the solvent under reduced pressure