HRID1995305

反应详情

EQUATION

反应方程式

HRID 1995305 的结构方程式

PROCEDURE

实验过程

Prepared by the method described for Example 13 from 1,2,3,4-tetrahydro-8-methoxy-5H-[1]benzopyrano[3,4-c]pyridin-5-one (3.0 g, 0.013 moles), triethylamine (7.2 ml, 0.052 moles), and 3-(2-chloroethyl)-3-azabicyclo-[3.3.1]nonane hydrochloride (3.25 g, 0.015 moles). Recrystallization from ethanol gave the product (2.4 g), mp 102°-103° C.

WORKUP

后处理

  1. customPrepared by the method
  2. customRecrystallization from ethanol