HRID2000308

反应详情

EQUATION

反应方程式

HRID 2000308 的结构方程式

REACTANTS

反应物

2

结构：NCc1ccccc1

Benzylamine

C7H9N

结构：CC(C)(C)OC(=O)N1CC[C@H]2O[C@H]2C1

tert-butyl (1S,6R)-7-oxa-3-azabicyclo[4.1.0]heptane-3-carboxylate

C10H17NO3

PRODUCTS

生成物

1

结构：CC(C)(C)OC(=O)N1CC[C@@H](NCc2ccccc2)[C@H](O)C1

tert-butyl (3R,4R)-4-(benzylamino)-3-hydroxypiperidine-1-carboxylate

C17H26N2O3

AUXILIARIES

试剂、催化剂与溶剂

3

结构：O=S(=O)([O-])C(F)(F)F.O=S(=O)([O-])C(F)(F)F.O=S(=O)([O-])C(F)(F)F.[Pr+3]

试剂HCID9894708

Praseodymium(III) trifluoromethanesulfonate

C3F9O9PrS3

结构：CC#N

Acetonitrile

C2H3N

结构：c1ccc(-c2c3ccccc3cc3ccccc23)cc1

内标HCID11766

9-Phenylanthracene

C20H14

CONDITIONS

反应条件

温度: 80 °C