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HRID2037

反应详情

EQUATION

反应方程式

HRID 2037 的结构方程式

REACTANTS

反应物

2
结构：ClCC1CC1
HCID80013

(Chloromethyl)cyclopropane

C4H7Cl

结构：CCOP(=O)(CCCn1c(=O)c2[nH]cnc2n(C)c1=O)OCC
HCID22446277

未命名化合物

PRODUCTS

生成物

1
结构：CCOP(=O)(CCCn1c(=O)c2c(ncn2CC2CC2)n(C)c1=O)OCC
HCID22446308

未命名化合物

PROCEDURE

实验过程

The title substance was prepared from 0.015 mol of diethyl [3-(3-methyl-xanthin-1-yl)propyl]phosphonate (Example 42), and 0.017 mol of chloromethylcyclopropane analogously to Example 30 and chromatographed on silica gel (eluent: dichloromethane/methanol 20:1).

WORKUP

后处理

  1. customchromatographed on silica gel (eluent: dichloromethane/methanol 20:1)