反应详情

温度

70 °C

To a solution of indoline 75 (8.5 g, 44.2 mmol) in MeOH (150 mL) was added α-D-glucose (27 g, 146 mmol) at room temperature. The mixture was stirred at 70° C. for 60 h, cooled to room temperature and concentrated in vacuo to remove solvent. The residue was purified by silica column chromatography to provide the titled compound 76 (13.7 g, 88%). MH+354.

1. temperaturecooled to room temperature
2. concentrationconcentrated in vacuo
3. customto remove solvent
4. customThe residue was purified by silica column chromatography