Chloride → HCID 12363407, compound

HRID 2051741Notes

Reaction equation

HRID 2051741 reaction equation
[Cl-].[Cl:2][C:3]1[CH:15]=[C:14]([O:16][CH3:17])[CH:13]=[CH:12][C:4]=1[O:5][CH2:6][CH2:7][O:8][CH2:9][CH2:10]Cl.[I-:18].[Na+]>CC(=O)CC>[Cl:2][C:3]1[CH:15]=[C:14]([O:16][CH3:17])[CH:13]=[CH:12][C:4]=1[O:5][CH2:6][CH2:7][O:8][CH2:9][CH2:10][I:18]

Participants

5

Reactant 3

HCID 312ChlorideHCID 5238Sodium IodideHCID 12363404HCID 12363404, compound

Product 1

HCID 12363407HCID 12363407, compound

Reagents, catalysts & solvents 1

HCID 6569Methyl Ethyl KetoneSolvent

Procedure

was prepared from 24.7 g. of the corresponding chloride of part (a) by three hours reflux with 13.5 g. of sodium iodide in 200 ml. of 2-butanone. The crude product was used directly in part (c) below.

Workup

  1. customwas prepared from 24.7 g

Sources & evidence

ORD record
ord-e444df19fb924eafbf9b75bfed3bf617
Source dataset
uspto-grants-1980_01
Patent number
US04182727

Reaction notes

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