Propylamine → HCID 54455417, compound

HRID 2051838Notes

Reaction equation

HRID 2051838 reaction equation
O=[CH:2][C@@H:3]([C@H:5]([C@@H:7]([CH2:9][OH:10])[OH:8])[OH:6])[OH:4].[CH2:11]([NH2:14])[CH2:12][CH3:13].[Cl:15][CH2:16][CH2:17][N:18]=[C:19]=[O:20]>>[Cl:15][CH2:16][CH2:17][NH:18][C:19]([N:14]([CH2:11][CH2:12][CH3:13])[CH:9]1[O:10][CH2:2][C@@H:3]([OH:4])[C@H:5]([OH:6])[C@H:7]1[OH:8])=[O:20]

Participants

4

Reactant 3

HCID 7852PropylamineHCID 160352-Chloroethyl isocyanateHCID 644160aldehydo-D-Xylose

Product 1

HCID 54455417HCID 54455417, compoundYield 67.5%

Procedure

3.0 g of D-xylose, 1.5 g of n-propylamine and 2.5 g of 2-chloroethyl isocyanate are treated in the same manner as described in Example 5-(1). 4.0 g of 1-(2-chloroethyl)-3-n-propyl-3-D-xylopyranosylurea are thereby obtained as colorless caramel.

Sources & evidence

ORD record
ord-384bb19c09e94aa0b07df637e040514d
Source dataset
uspto-grants-1980_01
Patent number
US04182757

Reaction notes

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