Sulfuric Acid → N-(Hexan-2-yl)prop-2-enamide

HRID 2051933Notes

Reaction equation

C(#N)C=C.CCCCC=C.[CH:11]1[C:24]2[NH:23][C:22]3C(=CC=[CH:20][CH:21]=3)S[C:15]=2[CH:14]=[CH:13][CH:12]=1.S(=O)(=O)(O)[OH:26]>>[CH3:15][CH:24]([NH:23][C:22](=[O:26])[CH:21]=[CH2:20])[CH2:11][CH2:12][CH2:13][CH3:14]

Participants

Reactant 4

HCID 1118Sulfuric Acid

HCID 7108Phenothiazine

HCID 7855Acrylonitrile

HCID 115971-Hexene

Product 1

HCID 20510138N-(Hexan-2-yl)prop-2-enamide

Procedure

Following a procedure analogous to that of Examples 1 and 2 from 530 pbw of acrylonitrile, 841.6 pbw hexene-1, 1.0 pbw phenothiazine and 1300 pbw 83% sulfuric acid, there is obtained 1010 pbw of the title product.

Sources & evidence

ORD record: ord-1bfd9c0e2cea402ea69d74a0295d029b
Source dataset: uspto-grants-1980_01
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04182790

Reaction notes

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