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HRID2052811

反应详情

EQUATION

反应方程式

HRID 2052811 的结构方程式

REACTANTS

反应物

3
结构：O=C([O-])[O-].[K+].[K+]
HCID11430

Potassium Carbonate

CK2O3

结构：COc1ccc(C(=O)CCl)cc1
HCID237806

2-Chloro-1-(4-methoxyphenyl)ethan-1-one

C9H9ClO2

结构：Cl.Cl.O=C(CN1CCNCC1)c1ccccc1
HCID23080512

1-Phenyl-2-(piperazin-1-yl)ethan-1-one--hydrogen chloride (1/2)

C12H18Cl2N2O

PRODUCTS

生成物

1
结构：COc1ccc(C(=O)CN2CCN(CC(=O)c3ccccc3)CC2)cc1.Cl.Cl
HCID131726748

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CN(C)C=O
溶剂HCID6228

N,N-Dimethylformamide

C3H7NO

PROCEDURE

实验过程

A mixture of 2-chloro-1-(4-methoxyphenyl)ethanone (3 mmol), N-phenacyl piperazine dihydrochloride (3 mmol) and K2CO3 (10 mmol) in 30 ml of DMF was treated according to the general preparation 2 to give compound (IV-9), 0.68 g (62%), mp 226-228° C., M+ 352.

WORKUP

后处理

  1. additionwas treated
  2. customaccording to the general preparation 2
  3. customto give compound (IV-9), 0.68 g (62%), mp 226-228° C., M+ 352