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HRID2052820

反应详情

EQUATION

反应方程式

HRID 2052820 的结构方程式

REACTANTS

反应物

3
结构：O=C([O-])[O-].[K+].[K+]
HCID11430

Potassium Carbonate

CK2O3

结构：O=C(CCl)NCc1ccc2c(c1)OCO2
HCID736835

N-(1,3-benzodioxol-5-ylmethyl)-2-chloroacetamide

C10H10ClNO3

结构：Cl.Cl.O=C(CN1CCNCC1)c1ccccc1
HCID23080512

1-Phenyl-2-(piperazin-1-yl)ethan-1-one--hydrogen chloride (1/2)

C12H18Cl2N2O

PRODUCTS

生成物

1
结构：Cl.Cl.O=C(CN1CCN(CC(=O)c2ccccc2)CC1)NCc1ccc2c(c1)OCO2
HCID86599628

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CC(C)=O
溶剂HCID180

Acetone

C3H6O

PROCEDURE

实验过程

A mixture of N-[1-(3,4-methylenedioxyphenyl)methyl]-2-chloroacetamide (5 mmol), N-phenacyl piperazine dihydrochloride (5 mmol) and K2CO3 (17.5 mmol) in 60 ml of acetone was treated according to the general preparation 2 to give compound (IV-32), 0.76 g (63.45%), M+ 395.

WORKUP

后处理

  1. additionwas treated
  2. customaccording to the general preparation 2
  3. customto give compound (IV-32), 0.76 g (63.45%), M+ 395