HRID2057913

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID70169

LS 75

C12H9N3O

HCID88014

6-Chlorohexanoyl chloride

C6H10Cl2O

PRODUCTS

生成物

结构：O=C1Nc2cccnc2N(C(=O)CCCCCCl)c2ccccc21

HCID15924302

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

溶剂HCID7237

o-Xylene

C8H10

PROCEDURE

实验过程

A solution of 5,11-dihydro-6H-pyrido-[2,3-b][1,4]-benzodiazepine-6-one and 6-chloro-caproyl chloride in xylene was reacted to obtain 11-(6-chloro-caproyl)-5,11-dihydro-6H-pyrido-[2,3-b][1,4]-benzodiazepine-6-one melting at 128°-130° C.