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HRID2059231

反应详情

EQUATION

反应方程式

HRID 2059231 的结构方程式

REACTANTS

反应物

2
结构：N#CCc1ccc(C(F)(F)F)cc1
HCID75359

4-(Trifluoromethyl)phenylacetonitrile

C9H6F3N

结构：COC(OC)N(C)C
HCID78373

Methanamine, 1,1-dimethoxy-N,N-dimethyl-

C5H13NO2

PRODUCTS

生成物

1
结构：CN(C)C=C(C#N)c1ccc(C(F)(F)F)cc1
HCID54490746

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：O
溶剂HCID962

Water

H2O

PROCEDURE

实验过程

4-(Trifluoromethyl)phenylacetonitrile (6.0 g.) in 5 ml. dimethylformamide-dimethylacetal was refluxed for 2 hours. Water was added and the final product was filtered, dried, and identified by NMR analysis.

WORKUP

后处理

  1. filtrationthe final product was filtered
  2. customdried