Benzaldehyde → HCID 69257954, compound

HRID 2061912Notes

Reaction equation

HRID 2061912 reaction equation
[CH:1](=O)[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[S:9]([NH2:13])([NH2:12])(=[O:11])=[O:10]>C(O)C>[NH2:12][S:9]([N:13]=[CH:1][C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1)(=[O:11])=[O:10]

Participants

4

Reactant 2

HCID 240BenzaldehydeHCID 82267Sulfamide

Product 1

HCID 69257954HCID 69257954, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

Benzaldehyde (5 g, 4 mmol) and sulfamide (9.06 g, 94 mmol) were dissolved in anhydrous ethanol (100 mL). The reaction mixture was heated to reflux for 2 hours then cooled to room temperature. The resulting solid was filtered and dried to yield the title compound.

Workup

  1. temperatureThe reaction mixture was heated
  2. temperatureto reflux for 2 hours
  3. filtrationThe resulting solid was filtered
  4. customdried

Sources & evidence

ORD record
ord-b8f5d73d634f46c2921bc003e7cd8791
Source dataset
uspto-grants-2012_10
Patent number
US08283478B2

Reaction notes

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