反应详情

A solution of (tetrahydro-2H-pyran-2-yl)methanol (1 g, 8.60 mmol) and di(1H-imidazol-1-yl)methanone (2.8 g, 17.2 mmol) in 17 mL CH2Cl2 was heated overnight at 50° C. The reaction was quenched with water, extracted with CH2Cl2, dried over MgSO4, filtered, and concentrated.

1. customThe reaction was quenched with water
2. extractionextracted with CH2Cl2
3. dry with materialdried over MgSO4
4. filtrationfiltered
5. concentrationconcentrated