Trifluoroacetic acid → HCID 68655173, compound

HRID 2063169Notes

Reaction equation

[F:1][C:2]([F:7])([F:6])[C:3]([OH:5])=[O:4].[NH2:8][CH2:9][CH2:10][N:11]1[CH2:16][CH2:15][NH:14][CH2:13][CH2:12]1>>[F:1][C:2]([F:7])([F:6])[C:3]([O-:5])=[O:4].[NH2:8][CH2:9][CH2:10][NH+:11]1[CH2:16][CH2:15][NH:14][CH2:13][CH2:12]1

Participants

Reactant 2

HCID 6422Trifluoroacetic acid2×

HCID 8795Aminoethylpiperazine

Product 1

HCID 68655173HCID 68655173, compound

Procedure

1-(2-aminoethyl)piperazinium trifluoroacetate was prepared in the same manner as Synthesis Example 1, except that 22.8 g (0.2 mol) of trifluoroacetic acid was added such that the molar ratio of 1-(2-aminoethyl)piperazine to trifluoroacetic acid was 1:2.

Sources & evidence

ORD record: ord-8e1d44394bab47e99c62cd34f6f27527
Source dataset: uspto-grants-2012_10
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US08287627B2

Reaction notes

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